Preparation of Mullite Powder by Corrosion Synthesis

Preparation of High Purity Mullite Ceramics

Nanocomposite mullite/mullite powders by spray pyrolysis

A mullite/mullite nanocomposite powder has been synthesized, composed of nanometer-size 3Al2O3 · 2SiO2 (‘3 : 2’) mullite precipitates within a matrix of the high alumina 2Al2O3 · SiO2 (‘2 : 1’) mullite. Historically, the transition from the metastable high-alumina phase to the thermodynamically stable ‘3 : 2’ phase of mullite has been thought to be a continuous process, involving a continuous s...

Preparation of nanostructured nickel aluminate spinel powder from spent NiO/Al2O3 catalyst by mechano-chemical synthesis

0921-8831/$ see front matter 2011 The Society of doi:10.1016/j.apt.2011.11.004 ⇑ Corresponding author. Address: School of Metallu ing, University of Tehran, P.O. Box 14395-1491, Tehran fax: +98 21 88006076. E-mail address: [email protected] (S. Sheibani). In this paper, the possibility of mechano-chemical synthesis, as a single step process for preparation of nanostructured nickel aluminate sp...

Synthesis & Characterization of CaB4O7 Powder by Solid-State Reaction

The synthesis of calcium tetraborate was investigated in a temperature ranging from 800℃ to 900℃ using the solid-state reaction method. The synthesis was done using ammonium tetraborate tetrahydrate as the source of boron. At temperatures of 800 ℃ and 880 ℃, the mixed phases from different compounds were formed. At the optimum temperature of 840℃, the mixed phase was only composed of meta and t...

New Method for Preparation of Nano Alumina Powder Using Aluminum(III) Complexes by Combustion Synthesis Without Fuel

Alumina nanomaterials were synthesized via a solution combustion technique using tris-(acetylacetonato) aluminum(III) complex (1) and tris-(2-formylphenolate) aluminum(III) complex (2) at 600, and 1000 °C for 3h. The obtained data showed that the procedure without using fuel resulted in a better phase and morphology. To investigate the phase formation, powder X-ray diffraction technique was use...